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Synthesis and biological profile of 2,3-dihydro[1,3]thiazolo[4,5- b ]pyridines, a novel class of acyl-ACP thioesterase inhibitors.
The present work covers novel herbicidal lead structures that contain a 2,3-dihydro[1,3]thiazolo[4,5- b ]pyridine scaffold as structural key feature carrying a substituted phenyl side chain. These new compounds show good acyl-ACP thioesterase inhibition in line with strong herbicidal activity against commercially important weeds in broadacre crops, e.g., wheat and corn. The desired substituted 2,3-dihydro[1,3]thiazolo[4,5- b ]pyridines were prepared via an optimized BH3 -mediated reduction involving tris(pentafluorophenyl)borane as a strong Lewis acid. Remarkably, greenhouse trials showed that some of the target compounds outlined herein display promising control of grass weed species in preemergence application, combined with a dose response window that enables partial selectivity in certain crops.
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