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Ordered Mesoporous NiCo 2 O 4 Nanospheres as a Novel Electrocatalyst Platform for 1-Naphthol and 2-Naphthol Individual Sensing Application.
ACS Applied Materials & Interfaces 2017 September 7
The novel ordered mesoporous NiCo2 O4 (meso-NiCo2 O4 ) nanospheres were synthesized by the nanocasting strategy followed by a calcination process for 2-naphthol (2-NAP) and 1-naphthol (1-NAP) individual sensing application. The as-obtained meso-NiCo2 O4 material possesses mesoporous structure in spinel crystalline type with a larger specific surface area than other structures. The meso-NiCo2 O4 -modified carbon paste electrode exhibited excellent electrocatalytic performance for NAP detection by amperometry measurement. The fabricated sensor of 2-NAP and 1-NAP has a wide linear detection range (0.02-300 and 0.02-20 μM) with high sensitivity (1.822 and 1.510 μA μM-1 cm-2 ) and low limit of detection (0.007 and 0.007 μM), respectively. In addition, the NAP sensors possess excellent reproducibility, stability, and selectivity.
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