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One pot synthesis of α-ketoamides from ethylarenes and amines: a metal free difunctionalization strategy.
Organic & Biomolecular Chemistry 2016 December 29
One-pot and metal free synthesis of α-ketoamides has been described through in situ generation of aryl ketones from easily available ethylarenes followed by amidation with various amines. This multiple oxidation protocol involves catalytic I2 -pyridine-TBHP (t-butyl hydroperoxide) mediated oxidative benzylic carbonylation and sequential NaI-TBHP mediated oxidative amidation without using any solvent.
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