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Highly nucleophilic vitamin B 12 -assisted nickel-catalysed reductive coupling of aryl halides and non-activated alkyl tosylates.
Chemical Communications : Chem Comm 2017 June 14
Reductive cross-coupling of aryl halides with ubiquitous alkyl tosylates was developed using a combination of nickel and vitamin B12 (VB12 : cyanocobalamin) catalysts. The tosylate was activated by reduced VB12 to form alkyl cobalt(iii), which served as a good alkylating agent for aryl-nickel species, leading to C(sp3 )-C(sp2 ) bond formation.
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