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Enantioselective Total Synthesis of the Neurotoxin Caramboxin.
Journal of Organic Chemistry 2024 April 13
Herein, we report the first and efficient asymmetric total synthesis of the neurotoxin (-)-caramboxin. The key to success is the creation of a stereogenic center by using enantioselective catalytic phase-transfer α-alkylation of glycine imines, affording this unusual α-amino acid in good yields and up to 99% ee. This work validates the S configuration of the natural product.
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