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Synthesis of 3,4,5-Trisubstituted 1,2,4-Triazoles via I 2 -Catalyzed Cycloaddition of Amidines with Hydrazones.
Journal of Organic Chemistry 2024 April 9
A general and practical method for the construction of various 3,4,5-trisubstituted 1,2,4-triazoles via I2 -catalyzed cycloaddition of N -functionalized amidines with hydrazones is reported. This strategy features cheap and readily available catalyst and starting materials, broader substrate scope, and moderate-to-good yields. The mechanism study shows that the existence of hydrogen on the nitrogen of hydrazones is crucial for this transformation.
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