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Mechanochemical carbon-carbon bond formation that proceeds via a cocrystal intermediate.

Stipe Lukin, Martina Tireli, Ivor Lončarić, Dajana Barišić, PrimoŽ Šket, Domagoj Vrsaljko, Marco di Michiel, Janez Plavec, Krunoslav UŽarević, Ivan Halasz
Chemical Communications : Chem Comm 2018 November 23
We report the first cocrystal as an intermediate in a solid-state organic reaction wherein molecules of barbituric acid and vanillin assume a favorable orientation for the subsequent Knoevenagel condensation.

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