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Diverse secondary C(sp 3 )-H bond functionalization via site-selective trifluoroacetoxylation of aliphatic amines.
Chemical Science 2018 August 15
We describe a coinage-metal-catalyzed site-selective oxidation of secondary C(sp3 )-H bonds for aliphatic amine substrates. Broad amine scope, good functional compatibility and late-stage diversification are demonstrated with this method. The steric demand of the β-substituents controlled diastereoselectivities under this catalytic system. The site selectivity favors secondary C(sp3 )-H bonds over tertiary ones underscoring the unique synthetic potential of this method.
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