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Synthesis of 28,28,28-trideutero-25-hydroxydihydrotachysterol 2 .
Journal of Steroid Biochemistry and Molecular Biology 2018 September 20
As part of our program on synthesis of labeled vitamin D metabolites and analogs, we describe here an efficient and versatile synthetic approach to 28,28,28-trideutero- 25-hydroxydihydrotachysterol2 where isotopic labeling was incorporated stereoselectively in the last step of the synthesis. This deuterated compound will allow the study this analog in vitro or in vivo and to measure AT10-like compounds in serum by LC-MS/MS.
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