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The selectively fluorescent sensing detection and adsorptive removal of Pb 2+ with a stable [δ-Mo 8 O 26 ]-based hybrid.
Journal of Colloid and Interface Science 2018 December 16
A polyoxomolybdate based hybrid, [δ-Mo8 O26 ](L)2 ·2H2 O (BUC-77), was synthesized via hydrothermal method, which exhibited selectively fluorescent detection and efficient adsorptive removal toward Pb2+ in aqueous environment. A good linearity was observed between the fluorescence quenching percentage of BUC-77 and the Pb2+ concentration, along with the detection limit being 6.91 ppb. BUC-77 was stable in common solvents and wide pH range, which could be regenerated by being washed with dilute inorganic acids like HNO3 after adsorption of Pb2+ . The results revealed that BUC-77 could be potentially used to achieve both detection and removal of Pb2+ in wastewater.
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