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A ruthenium-catalyzed alkenylation-annulation approach for the synthesis of indazole derivatives via C-H bond activation.
Organic & Biomolecular Chemistry 2018 August 23
Ruthenium catalyzed oxidative alkenylation of N-aryl pyridazinediones and N-aryl phthalazinediones with acrylates and subsequent intramolecular cyclization of the resulting product in water as a green solvent were accomplished. Diverse derivatives of pyridazino[1,2-a]indazoles and indazolo[1,2-b]phthalazines were readily prepared in moderate to high yields by this methodology from easily accessible starting materials via cascade directed C-H bond activation/annulation reactions.
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