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Retention of a Paramagnetic Ground State at Low Temperatures in a Family of Structurally Related U IV Phosphates.
Inorganic Chemistry 2018 August 7
A new uranium fluoride phosphate, UFPO4 , was synthesized via a mild hydrothermal route and characterized optically, thermally, and magnetically. Two thermal transformation products, U2 O(PO4 )2 and UIV UVI O2 (PO4 )2 , were discovered to be structurally related, and were subsequently synthesized for bulk property measurements. All three materials failed to follow Curie-Weiss behavior at low temperatures, attributed to the nearly ubiquitous singlet ground state of U(IV), transitioning into a Curie-Weiss paramagnetic regime at high temperatures. Neutron diffraction experiments were performed on UFPO4 and UIV UVI O2 (PO4 )2 in order to characterize this unusual magnetic behavior.
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