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RESEARCH SUPPORT, N.I.H., EXTRAMURAL
RESEARCH SUPPORT, NON-U.S. GOV'T
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Total Synthesis and Biological Activity of the Arachidonic Acid Metabolite Hemiketal E 2 .

Robert E Boer, Juan Antonio Giménez-Bastida, Olivier Boutaud, Somnath Jana, Claus Schneider, Gary A Sulikowski
Organic Letters 2018 July 7
The total synthesis of hemiketal E2 (HKE2 ) has been accomplished using a gold(I)-mediated cycloisomerization followed by oxidation of the enol ether product to introduce a unique keto-hemiketal, the core structure of HKE2 . Synthetic hemiketal E2 reproduced biosynthetically derived HKE2 in the inhibition of human platelet aggregation.

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