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Synthesis of CF 3 -containing spiro-epoxyoxindoles via the Corey-Chaykovsky reaction of N-alkyl isatins with Ph 2 S + CH 2 CF 3 OTf .
Organic & Biomolecular Chemistry 2018 May 16
CF3-containing spiro-epoxyoxindoles were successfully prepared via the Corey-Chaykovsky reaction of N-alkyl isatins with the ylide generated from Ph2S+CH2CF3OTf- with almost exclusive diastereoselectivity. Further derivatizations of these spiro-epoxyoxindoles were explored via a photochemical reaction or Lewis acid-promoted allylation.
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