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Journal Article
Research Support, Non-U.S. Gov't
A Concise Approach to Anthraquinone-Xanthone Heterodimers.
Journal of the American Chemical Society 2018 April 19
A synthetic approach to anthraquinone-xanthone heterodimers is described. The route to the pentacyclic core features an efficient assembly of a benzocycloheptenone via a new intramolecular oxidative arylation of an enol ether and a Hauser-Kraus annulation-aldol reaction sequence to access the characteristic bicyclo[3.2.2]nonene motif. Acremoxanthone A is synthesized in 10 steps from commercially available material to demonstrate the application of this approach.
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