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JOURNAL ARTICLE
RESEARCH SUPPORT, NON-U.S. GOV'T
One-Step Synthesis of Aliphatic Potassium Acyltrifluoroborates (KATs) from Organocuprates.
Organic Letters 2018 April 21
A one-step synthesis of aliphatic KATs from organocuprates is reported. Organolithium and organomagnesium reagents were readily transmetalated onto Cu(I) and coupled with a KAT-forming reagent to yield the respective aliphatic KAT. The protocol is suitable for primary, secondary and-for the first time-tertiary alkyl substrates. These protocols considerably expand the range of KATs that can be readily accessed in one step from commercially available starting materials.
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