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Na 2 (UO 2 )(BO 3 ): An All-Uranium(V) Borate Synthesized under Mild Hydrothermal Conditions.

Kristen A Pace, Vancho Kocevski, Stavros G Karakalos, Gregory Morrison, Theodore Besmann, Hans-Conrad Zur Loye
Inorganic Chemistry 2018 April 17
The first entirely pentavalent uranium borate, Na2 (UO2 )(BO3 ), was synthesized under mild hydrothermal conditions. The single-crystal structure was solved in the orthorhombic space group Cmcm with a = 10.0472(3) Å, b = 6.5942(2) Å, and c = 6.9569(2) Å. Magnetic susceptibility measurements revealed an antiferromagnetic transition at 12 K and an effective magnetic moment of 2.33 μB . Density functional theory calculations indicated dynamic stability of the structure above 0 K.

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