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Journal Article
Research Support, Non-U.S. Gov't
An Orchestrated Unsymmetrical Annulation Episode of C(sp 2 )-H Bonds with Alkynes and Quinones: Access to Spiro-isoquinolones.
Organic Letters 2018 April 7
A nontrivial Ru-catalyzed one-pot sequential oxidative coupling of a (hetero)arene/vinylic/chromene system with alkyne and quinone is presented; the methyl phenyl sulfoximine (MPS) directing group is vital. This cyclization forms four (two C-C and two C-N) bonds in a single operation and produces unusual spiro-fused-isoquinolones with a broad scope. The release of phenyl methyl sulfoxide makes the MPS group transformable. A deuterium scrambling study sheds light on the reaction path.
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