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Synthesis and HNO Donating Properties of the Piloty's Acid Analogue Trifluoromethanesulphonylhydroxamic Acid: Evidence for Quantitative Release of HNO at Neutral pH Conditions.

Sonya K Adas, Vinay Bharadwaj, Yang Zhou, Jiuhong Zhang, Alexander J Seed, Nicola E Brasch, Paul Sampson
Chemistry : a European Journal 2018 May 24
Trifluoromethanesulphonylhydroxamic acid, CF3 SO2 NHOH, is shown to release HNO under physiological pH conditions. A two-step synthesis is presented with the first complete characterization of CF3 SO2 NHOH. This molecule rapidly decomposes in neutral aqueous solution to cleanly release HNO and CF3 SO2 - , which was demonstrated using the HNO traps TXPTS and HOCbl, and by 19 F NMR spectroscopy.

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