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Unravelling Lawesson's reagent: the structure of monomeric (4-methoxyphenyl)phosphine disulfide.
Chemical Communications : Chem Comm 2018 March 14
We describe the isolation as well as IR and UV/Vis spectroscopic characterization of (4-methoxyphenyl)phosphine disulfide in argon matrices at 10 K. The title compound proved to be highly photolabile; irradiation with UV light (λ = 334 nm) led to rearrangement to the equally unreported 3-(4-methoxyphenyl)-1,2,3-dithiaphosphirane. Photoreversion can be achieved upon irradiation at λ = 465 nm.
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