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Journal Article
Research Support, Non-U.S. Gov't
Visible-Light-Enabled Preparation of Palladium Nanoparticles and Application as Catalysts for Suzuki-Miyaura Coupling.
Organic Letters 2018 Februrary 3
Silyl ketones were used for the preparation of palladium nanoparticles (PdNPs) starting with Pd(OAc)2 in dimethylformamide under irradiation with a visible light-emitting diode (LED). Variation of the silyl ketone structure allowed adjustment of the PdNP diameter (1.9 or 5.2 nm). The in situ-formed PdNPs were further stabilized with polyvinylpyrrolidone and then applied as recyclable catalysts in the Suzuki-Miyaura coupling of arylboronic acids with aryl iodides to obtain substituted biphenyls in excellent yields.
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