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Journal Article
Research Support, Non-U.S. Gov't
Catalytic Oligopeptide Synthesis.
Organic Letters 2018 Februrary 3
Waste-free catalytic assembly of α-amino acids is fueled by a multiboron catalyst that features a characteristic B3 NO2 heterocycle, providing a versatile catalytic protocol wherein functionalized natural α-amino acid units are accommodated and commonly used protecting groups are tolerated. The facile dehydrative conditions eliminate the use of engineered peptide coupling reagents, exemplifying a greener catalytic alternative for peptide coupling. The catalysis is sufficiently robust to enable pentapeptide synthesis, constructing all four amide bond linkages in a catalytic fashion.
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