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Research Support, N.I.H., Extramural
Research Support, U.S. Gov't, Non-P.H.S.
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Synthesis of Cyclic Enones by Allyl-Palladium-Catalyzed α,β-Dehydrogenation.

David Huang, Yizhou Zhao, Timothy R Newhouse
Organic Letters 2018 Februrary 3
The use of allyl-palladium catalysis for the one-step α,β-dehydrogenation of ketones via their zinc enolates is reported. The optimized protocol utilizes commercially available Zn(TMP)2 as base and diethyl allyl phosphate as oxidant. Notably, this transformation operates under salt-free conditions and tolerates a diverse scope of cycloalkanones.

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