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Journal Article
Research Support, Non-U.S. Gov't
Role of Ring Ortho Substituents on the Configuration of Carotenoid Polyene Chains.
Organic Letters 2018 January 20
The 9-(Z)-configuration was exclusively obtained in the carotenoid polyene chain irrespective of olefination and disconnection methods for terminal ortho-unsubstituted benzene rings. The 2,6-dimethyl substituents in the terminal rings secure an all-(E)-polyene structure. The single molecular conductance of the pure 9-(Z)-carotene was measured for the first time to be 1.53 × 10-4 ± 6.37 × 10-5 G0 , whose value was 47% that of the all-(E)-carotene ((3.23 × 10-4 ) ± (1.23 × 10-4 ) G0 ).
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