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JOURNAL ARTICLE
RESEARCH SUPPORT, NON-U.S. GOV'T
Rh(II)-Catalyzed Chemoselective Oxidative Amination and Nucleophilic Trapping of gem-Dimethyl Alkynyl-Tethered Sulfamates.
Organic Letters 2018 January 6
A Rh(II)-catalyzed chemoselective oxidative amination and nucleophilic trapping of gem-dimethyl sulfamates has been presented. For 2,2-dimethyl-4-arylbut-3-yn-1-yl sulfamates, the reactions underwent a metallonitrene-initiated alkyne oxidation along with nucleophilic trapping of H2 O upon oxidation, giving aroyl group containing heterocycles. For 2,2-dimethyl-4-arylpent-3-yn-1-yl sulfamates, the α-iminometal carbene intermediate was trapped by aryl group migration, delivering a styryl group containing heterocycles.
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