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Journal Article
Research Support, Non-U.S. Gov't
Direct Activation of β-sp 3 -Carbons of Saturated Carboxylic Esters as Electrophilic Carbons via Oxidative Carbene Catalysis.
Organic Letters 2018 January 6
An N-heterocyclic carbene-catalyzed oxidative LUMO activation of the β-cabons of saturated carboxylic esters is disclosed. This approach allows for efficient asymmetric access to lactams and lactones by directly installing functional groups to the typically inert β-sp3 carbons of saturated esters. The use of HOBt as an additive was found to significantly improve both yields and enantioselectivities of the reactions.
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