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JOURNAL ARTICLE
RESEARCH SUPPORT, NON-U.S. GOV'T
Synthesis of 3-(Arylsulfonyl)benzothiophenes and Benzoselenophenes via TBHP-Initiated Radical Cyclization of 2-Alkynylthioanisoles or -selenoanisoles with Sulfinic Acids.
Organic Letters 2017 December 2
tert-Butyl hydroperoxide-initiated radical cyclization of 2-alkynylthioanisoles or -selenoanisoles with sulfinic acids has been developed. This reaction is applicable to a wide substrate scope via one C(sp3 )-S(Se) bond cleavage and two C(sp2 )-S(Se) bond formation, leading to the synthesis of 3-(arylsulfonyl)benzothiophenes or -benzoselenophenes under mild conditions.
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