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Amidoboranes of rubidium and caesium: the last missing members of the alkali metal amidoborane family.

We report the synthesis and physicochemical characterization of two ammonia borane derivatives: rubidium amidoborane (RbNH2 BH3 ) and caesium amidoborane (CsNH2 BH3 ). Both compounds undergo solid-solid phase transition upon heating and then evolve pure hydrogen at temperatures lower than 125 °C. The phase transition is clearly seen in the Raman spectra. We present crystal structures of both low- and high-temperature forms of the title compounds which were solved from powder X-ray data.

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