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JOURNAL ARTICLE
RESEARCH SUPPORT, NON-U.S. GOV'T
Total Synthesis of (-)-Geissoschizol through Ir-Catalyzed Allylic Amidation as the Key Step.
Organic Letters 2017 December 2
The iridium-catalyzed, Zn(OTf)2 promoted asymmetric allylic amidation of a secondary alcohol derived from tryptamine has been utilized to forge a tetrahydro-β-carboline. Based on this key step, a novel, facile, and enantioselective total synthesis of (-)-geissoschizol was achieved in 10 steps.
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