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Journal Article
Research Support, Non-U.S. Gov't
Research Support, U.S. Gov't, Non-P.H.S.
Crystalline Monomeric Allenyl/Propargyl Radical.
Journal of the American Chemical Society 2017 November 9
Reduction of alkynyl iminium salts derived from cyclic (alkyl)(amino)carbenes (CAACs) affords propargyl/allenyl radicals. Depending on the nature of the CAAC and alkyne substituents, these radicals can irreversibly dimerize, exist as monomers in solution but dimerize in the solid state, or can even remain monomeric as solids. The first characterization of an allenyl radical by single crystal X-ray crystallography is reported.
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