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JOURNAL ARTICLE
RESEARCH SUPPORT, NON-U.S. GOV'T
Chiral Nanographene Propeller Embedding Six Enantiomerically Stable [5]Helicene Units.
Journal of the American Chemical Society 2017 December 28
A one-step synthesis of a nanographene propeller with a D3 -symmetry was obtained starting from 7,8-dibromo[5]helicene by Yamamoto nickel(0) couplings. It afforded a chiral polyaromatic hydrocarbon (PAH) embedding six enantiomerically stable [5]helicene units. This dense accumulation of helical strain resulted in a distorted geometry, but stable stereochemistry. The conformational, structural, chiroptical, and photophysical properties of the molecule are reported.
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