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Non-order-disorder allotwinning of the rhenium pincer complex cis-Re[(PNP CH 2 -iPr)(CO) 2 Cl].
Acta Crystallographica Section B, Structural Science, Crystal Engineering and Materials 2017 October 2
Crystals of cis-Re[(PNPCH2 -iPr)(CO)2 Cl] (1) are made up of two geometrically non-equivalent polytypes with respective symmetries of P21 /c and I2/a. The structures were determined in a concurrent refinement, taking into account overlap of diffraction spots. The polytypes are composed of layers with px 121 /c1 symmetry and are of the non-order-disorder (OD) type (the layer interfaces are non-equivalent). Whereas the molecules of (1) differ in both polytypes, the Re atoms are located at nearly identical positions.
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