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Well-defined silica supported bipodal molybdenum oxo alkyl complexes: a model of the active sites of industrial olefin metathesis catalysts.
Chemical Communications : Chem Comm 2017 October 13
A well-defined, silica-supported molybdenum oxo alkyl species, ([triple bond, length as m-dash]SiO-)2 Mo([double bond, length as m-dash]O)(CH2 t Bu)2 , was prepared by the selective grafting of Mo([double bond, length as m-dash]O)(CH2 t Bu)3 Cl onto a silica partially dehydroxylated at 200 °C using a rigorous surface organometallic chemistry approach. The immobilized bipodal surface species, partly resembling the active species of industrial MoO3 /SiO2 olefin metathesis catalysts, exhibited excellent functional group tolerance in conjunction with its high activity in homocoupling, self and ring closing olefin metathesis.
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