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JOURNAL ARTICLE
RESEARCH SUPPORT, NON-U.S. GOV'T
Trifluoromethylthiolation-Based Bifunctionalization of Diazocarbonyl Compounds by Rhodium Catalysis.
Organic Letters 2017 September 2
A new Rh-catalyzed, three-component reaction for the oxytrifluoromethylthiolation of α-diazoketones was developed. The SCF3 functionality was introduced using a stable dibenzenesulfonimide reagent under mild conditions. Alcohols, acetals, and ethers were used as the alkoxy sources. Cyclic ethers underwent a trifunctionalization reaction through the introduction of SCF3 , OR, and N(SO2 Ph)2 substituents in a single step.
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