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Journal Article
Research Support, Non-U.S. Gov't
Nonepimerizing Alkylation of H-P Species to Stereospecifically Generate P-Stereogenic Phosphine Oxides: A Shortcut to Bidentate Tertiary Phosphine Ligands.
Journal of Organic Chemistry 2017 September 16
The secondary RP -(-)-menthyl alkylphosphine oxide was confirmed as configurationally stable toward base and was used in base-promoted alkylation, stereospecifically affording P-retained bis or functional tertiary phosphine oxides in excellent yields. The alkylated products were deoxygenated using oxalyl chloride followed by ZnCl2 -NaBH4 to form P-inversed bidentate phosphine boranes in high stereoselectivities.
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