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Asymmetric alkylation of remote C(sp 3 )-H bonds by combining proton-coupled electron transfer with chiral Lewis acid catalysis.
Chemical Communications : Chem Comm 2017 August 9
The catalytic asymmetric alkylation of the remote, unactivated δ-position of N-alkyl amides was enabled by the combination of visible-light-induced proton-coupled electron transfer, 1,5-hydrogen atom transfer, and chiral Lewis acid catalysis in up to 82% yield and up to 97% ee.
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