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Deep-Ultraviolet Nonlinear-Optical Material K 3 Sr 3 Li 2 Al 4 B 6 O 20 F: Addressing the Structural Instability Problem in KBe 2 BO 3 F 2 .

Inorganic Chemistry 2017 August 8
A beryllium-free deep-ultraviolet (DUV) nonlinear-optical (NLO) material, K3 Sr3 Al4 Li2 B6 O20 F, has been synthesized and characterized. Unlike KBe2 BO3 F2 (KBBF), the reported NLO material does not require the use of toxic BeO in the synthesis, and through the judicious selection of cations, strong interlayer interactions are observed that facilitate the crystal growth. K3 Sr3 Al4 Li2 B6 O20 F exhibits second-harmonic generation (SHG) at both 1064 and 532 nm with efficiencies of 1.7KH2 PO4 and 0.3β-BaB2 O4 and has an absorption edge of 190 nm. Because of the strong interlayer interactions, we were able to grow well-faceted large crystals, 8 × 8 × 5 mm3 , through a top-seeded-solution-growth technique. With these crystals, we determined a birefringence of 0.0574 at 1064 nm and a type I phase-matching SHG limit of 224 nm.

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