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Stereoselective synthesis of 25S,26-dihydroxyvitamin D 3 .

Rita Sigüeiro, Patricia González-Berdullas, Julian Loureiro, Antonio Mouriño, Miguel A Maestro
Journal of Steroid Biochemistry and Molecular Biology 2018 March
A convergent approach to 25S,26-dihydroxyvitamin D3 (1) has been developed in our laboratories. The A-ring and the CD-fragment are constructed from ergocalciferol and Inhoffen-Lythgoe diol, respectively. The triene system is assembled by a Wittig-Horner coupling. With this convergent synthesis, a novel hydroxylated vitamin D metabolite in our laboratory is available for biological testing.

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