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JOURNAL ARTICLE
RESEARCH SUPPORT, NON-U.S. GOV'T
Electrochemical Nickel Catalysis for Sp 2 -Sp 3 Cross-Electrophile Coupling Reactions of Unactivated Alkyl Halides.
Organic Letters 2017 July 22
A constant-current electrochemical method for reducing catalytic nickel complexes in sp2 -sp3 cross-electrophile coupling reactions has been developed. The electrochemical reduction provides reliable nickel catalyst activation and turnover and offers a tunable parameter for reaction optimization, in contrast to more standard activated metal powder reductants. The electrochemical reactions give yields (i.e., 51-86%) and selectivities as high or superior to those using metal powder reductants and provide access to a wider substrate scope.
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