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Journal Article
Research Support, Non-U.S. Gov't
Total Synthesis of the Cyclic Dodecapeptides Wewakazole and Wewakazole B.
Organic Letters 2017 July 8
The cyclic dodecapeptides wewakazole and wewakazole B have been synthesized by a divergent strategy via a common tris-proline containing oxazole octapeptide and two separate bis-oxazole containing tetrapeptide units, followed by peptide coupling and macrocyclization. The three oxazole amino acid fragments are readily accessible by rhodium(II)-catalyzed amide N-H insertion of diazocarbonyl compounds, or by the cycloaddition of rhodium carbenoids with nitriles.
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