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JOURNAL ARTICLE
RESEARCH SUPPORT, NON-U.S. GOV'T
Organocatalytic Enantioselective Michael-Acetalization-Reduction-Nef Reaction for a One-Pot Entry to the Functionalized Aflatoxin System. Total Synthesis of (-)- Dihydroaflatoxin D 2 and (-)- and (+)-Microminutinin.
Organic Letters 2017 July 8
An efficient method has been developed for the enantioselective synthesis of the aflatoxin system with multiple stereocenters via a sequence of organocatalytic Michael-acetalization-reduction-Nef reactions that proceed with high enantioselectivities (90-99% ee). The one-pot reaction sequence provides a facile entry to the aflatoxin system, including dihydroaflatoxin D2 , which includes a formal total synthesis of aflatoxin B2 . The first total synthesis of (-)- and (+)-microminutinin was also achieved via this protocol.
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