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Unprecedented Carbon Signal Enhancement in Liquid-State NMR Spectroscopy.
Angewandte Chemie 2017 July 11
We shall overcome: As a result of efforts to overcome the sensitivity challenge of liquid-state NMR spectroscopy, a thousand-fold signal enhancement was achieved by dynamic nuclear polarization (DNP) for (13) C signals at high magnetic field (3.4 T) and room temperature, thereby exceeding the predicted limitations of high-field liquid-state in situ DNP.
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