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JOURNAL ARTICLE
RESEARCH SUPPORT, NON-U.S. GOV'T
Radical Silyldifluoromethylation of Electron-Deficient Alkenes.
Organic Letters 2017 June 17
A reaction of bromo- and iododifluoromethyl-substituted silanes with electron-deficient alkenes in the presence of an N-heterocyclic carbene borane complex is described. The reaction is performed under irradiation with light-emitting diodes and proceeds via a radical chain mechanism. The resulting products, the functionalized silicon reagents, can undergo chemoselective transformations involving either the silyldifluoromethyl fragment or the functional group.
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