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JOURNAL ARTICLE
RESEARCH SUPPORT, NON-U.S. GOV'T
Formal Total Synthesis of (±)-Lycojaponicumin C.
Organic Letters 2017 June 3
The formal total synthesis of (±)-lycojaponicumin C has been accomplished. Key transformations include a Rh-catalyzed formal [3 + 2] cycloaddition reaction to construct the bicyclic [3.3.0] scaffold bearing two vicinal quaternary carbon centers, a stereoselective γ-hydroxyl directed Michael addition to introduce the vinyl group at a bulky position, and a late-stage ring-closing metathesis reaction to form the cyclohexanone ring.
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