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Iodine-mediated synthesis of sulfur-bridged enaminones and chromones via double C(sp 2 )-H thiolation.
Organic & Biomolecular Chemistry 2017 May 32
The reactions of various enaminones with elemental sulfur giving rise to both sulfur-bridged enaminones and chromones have been realized via iodine promotion. All products were furnished by means of double C(sp2 )-H bond thiolation without using any metal catalyst or sensitive oxidant, providing a simple and efficient protocol for the synthesis of diverse sulfur derivatives of enaminones.
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