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Synthesis and activation potential of an open shell diphosphine.

Kai Helmdach, Stephan Ludwig, Alexander Villinger, Dirk Hollmann, Jutta Kösters, Wolfram W Seidel
Chemical Communications : Chem Comm 2017 May 31
A paramagnetic WIII alkyne complex bearing free terminal diphenylphosphino groups at the side-on coordinated alkyne was synthesized using a stepwise template strategy. This moderately stable metal supported open shell diphosphine shows an unprecedented spontaneous splitting of nitric oxide providing a WII -η2 -C2 {P(NH2 )Ph2 }{P(O)Ph2 }+ complex featuring an amino phosphonium and a phosphine oxide substituent.

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