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Zinc hydridotriphenylborates supported by a neutral macrocyclic polyamine.
The zinc hydridotriphenylborates [(L)Zn(TMDS)][HBPh3 ] and [(L)ZnX][HBPh3 ] (L = Me4 TACD, Me4 [12]aneN4 ; TMDS = N(SiHMe2 )2 ; X = Cl, Br, I) were synthesized by BPh3 -mediated β-SiH abstraction and salt metathesis with KHBPh3 , respectively. CO2 is rapidly inserted into the B-H bonds. [(L)Zn(TMDS)][HBPh3 ] catalyzes the hydroboration of polar substrates including CO2 .
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