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JOURNAL ARTICLE
RESEARCH SUPPORT, NON-U.S. GOV'T
Cp*Co(III)-Catalyzed Annulation of Carboxylic Acids with Alkynes.
Organic Letters 2017 May 20
A new procedure for oxidative coupling of aromatic and acrylic acids with alkynes has been developed using abundant, nontoxic, and air stable Cp*Co(III) catalyst. The coupling involves initial cyclometalation via weak chelation-assisted C-H bond activation followed by alkyne coordination, insertion, and reductive elimination leading to diverse isocoumarins (α-pyranones) in good yields under mild conditions.
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