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Journal Article
Research Support, Non-U.S. Gov't
Stereoselective Total Synthesis of Carolacton.
Organic Letters 2017 May 6
A short and convergent strategy for the stereoselective total synthesis of biologically active natural product carolacton has been accomplished. Our synthesis highlights the Urpi acetal aldol, Crimmins aldol, Ireland-Claisen rearrangement, TiCl4 -assisted aldol followed by β-hydroxy elimination to construct C7 -C8 olefin, and ring-closing metathesis as the key steps for achieving the target molecule with an overall yield of 18.8%.
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