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A macrocyclic 'Co 0 ' complex: the relevance of ligand non-innocence to reactivity.
Chemical Communications : Chem Comm 2017 June 30
We present a formally zero-valent compound, [Co(Mabiq)Na(OEt2 )]2 (1). The complex was characterized by crystallographic, spectroscopic and DFT computational methods. The electronic structure is described as a CoII -(ligand-biradical). Compound 1 is reactive toward proton sources; CoI or CoII products result, depending on the source of protons used. The redox non-innocence of the Mabiq ligand, which accepts both protons and electrons, has important ramifications for reactivity.
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